Introduction: The continuous flow microwave system is usually suitable for rapid heating (physical process) and flow-dynamic synthesis extraction reaction (chemical process) through the microwave electromagnetic field environment in a liquid-phase continuous flow mode under the micro-positive pressure state of the material pump; suitable for chemical processes Scientific research (synthetic organic chemistry, inorganic chemistry, analytical chemistry, medicinal chemistry, military chemistry), biomedicine, material science, food science, inspection and quarantine, petrochemical and agriculture, forestry and fishery testing fields; microwave continuous flow process, precise process control, stable performance , it is easy to realize industrialization through series-parallel mode. Features: 1. Microwave continuous flow chemical reaction platform, suitable for continuous pipeline disposal process of liquid fluid materials 2. Adopt 20L stainless steel chemical anti-corrosion cavity design, microwave power 800W 3. Built-in engineering plastic reaction coil system, diameter Φ6mm (Φ1～Φ10 optional) 4. Microwave reaction pressure control: 0～0.5MPa (0～2MPa optional) 5. Microwave reaction temperature control: 0～100˚C (0～200˚C optional) 6. Support four-port pipeline system, parallel, confluence and split modes are optional 7. It supports the dual liquid dynamic process mode of external circulation and internal circulation, and the flow range is 0～1000ml/min 8. Support dynamic sampling function of flow dynamic reaction material 9. Intelligent control system, closed-loop control of temperature, pressure and power, support for staged heating process and temperature compensation process 10. The experimental data curve is displayed and the data can be exported 11. Safety system: (1) Electrical interlock (2) Temperature monitoring (3) Pressure monitoring (4) Microwave leakage prevention and suppression Technical parameter: microwave system 1. Microwave power control: ①Microwave power: rated power 800W, linearly adjustable from 0 to 800W, stepless non-pulse continuous microwave power output ②Microwave frequency: 2450±50MHz 2. Design of microwave reaction cavity: ①304 stainless steel is welded together, which is strong and reliable; ②The inner surface is coated with 5 layers of Teflon anti-corrosion coating, which is suitable for use in environments with acid and alkali corrosion and high temperature, and is easy to wipe and clean 3. Inner cavity size: about 20L, 250×275×285mm (width×height×depth), the height of 275mm is designed for the installation and pick-up of various reactors functional system 1. Reaction system: choose Φ60✕10000mm engineering plastic piping system, support temperature measurement, pressure measurement, flow function, (engineering plastic reaction system of different materials and specifications can be selected) 2. Temperature control: common working temperature is 0～100℃, support optional maximum temperature of 200℃ 3. Pressure control: the common pressure range is 0~0.5MPa, and the maximum pressure is 2MPa. 4. Fluid control: design a four-port piping system, using the internal circulation and external circulation dual-fluid mode 5. Process monitoring: ①The interior of the microwave cavity is equipped with LED spotlights, and the working conditions in the furnace cavity are monitored through the observation window of the door body ②Set up color video to monitor the reaction of internal materials, and you can understand the working status of the reaction system through the video Control System 1. Using PLC programming control: good human-computer interaction, integrated control terminal, temperature, pressure and power are intelligently controllable 2. Touch screen dialogue window, easy and fast operation, real-time display of time, temperature, power curve 3. Multiple sets of program memory functions, which can store, modify, call, delete and other system operations on the program, can read the data during the experiment, and analyze and edit through the computer security system 1. The door body has multiple interlocking structure, the door is powered off, and the operator is protected 2. The door body adopts a pull-down buckle locking structure, which ensures the strong locking state of the furnace door through metal connection; at the same time, the door body is embedded with an elastic translation pressure relief structure, which can release pressure from both sides under the condition of abnormal reaction and runaway to protect the front. operator. 3. The inside of the door body adopts a high-impedance microwave anti-current suppression structure to ensure the health and safety of operators. Microwave leakage: <5mw/cm2 (better than the national standard) 4. A moisture exhaust fan is installed on the back plate of the furnace cavity, which can quickly remove the exhaust gas in the furnace cavity, ensure a slightly negative pressure environment in the furnace cavity, and protect the operators Machine description 1. Use environment: (1) Non-flammable and explosive environment; (2) Humidity 15-80%; (3) Ambient temperature: 5-40˚C 2. Equipment power supply: 220Vac / 50Hz, power consumption of the whole machine: 1300W 3. Appearance size: main body about: 782×492×450mm (width×height×depth) 4. Equipment weight: 50kg
Introduction: The continuous flow microwave system is usually suitable for rapid heating (physical process) and flow-dynamic synthesis extraction reaction (chemical process) through the microwave electromagnetic field environment in a liquid-phase continuous flow mode under the micro-positive pressure state of the material pump; suitable for chemical processes Scientific research (synthetic organic chemistry, inorganic chemistry, analytical chemistry, medicinal chemistry, military chemistry), biomedicine, material science, food science, inspection and quarantine, petrochemical and agriculture, forestry and fishery testing fields; microwave continuous flow process, precise process control, stable performance , it is easy to realize industrialization through series-parallel mode.
