Introduction: The instrument adopts microwave non-pulse continuous automatic frequency conversion control to extend the service life of the instrument and the uniformity of electromagnetic waves. The cavity is made of 52L large volume 316L stainless steel cavity material, and the self-locking buffer explosion-proof furnace door, when the reaction is abnormal, The buffer structure ensures the operator's personal safety and the structure of the furnace door is intact, the furnace door and the cavity are tightly combined, and the microwave leakage complies with national standards. The instrument uses a temperature and pressure dual control system to control the pressure and temperature of the synthesis experiment and display it in real time. The 360° round-trip continuous rotation and uniform microwave ensure the same microwave environment of each sample and improve the consistency of experimental results. When the pressure in the tank exceeds the set protection value, the microwave will automatically stop heating. The safety explosion-proof membrane has a double safety function. When the pressure inside the tank exceeds the pressure that the explosion-proof membrane can withstand, the explosion-proof membrane first ruptures, and the gas vents to prevent damage to the tank and damage to the human body. Technical Parameters: 1. Power output mode: microwave non-pulse continuous automatic frequency conversion control. 2, output power: 1400W automatic continuous adjustable; 3, high-precision platinum resistance temperature sensor, temperature control: 0 ~ 300 ° C; temperature control accuracy: ± 0.5 ° C; with the rate of temperature heating required for microwave synthesis. 4, the maximum use temperature: 300 ° C; 5, pressure control range: 0 ~ 6MPa, the highest pressure 15MPa, pressure control accuracy: 0.01MPa; 6, 360 ° round-trip continuous rotation, microwave uniformity, to ensure the same microwave environment of each sample, improve the consistency of experimental results. 7, 8 inch touch screen liquid crystal display, touch operation, real-time display of closed reaction tank temperature, pressure, and real-time display of temperature and pressure curve. 8, 52L large volume 316L stainless steel cavity, 6 layers of anti-corrosion PFA Teflon inside and outside. Corrosion resistant and high temperature resistant. 9. The volume is 100ml microwave synthesis tank, the outer tank adopts imported PEEK aerospace material, and the inner tank is PTFE material; 10. The main tank is connected to the temperature and pressure, and the auxiliary tank is tightly sealed with a ceramic plug for the explosion-proof membrane. The temperature of the ceramic plug is not deformed. 11. High-throughput sample synthesis, up to 12 samples can be synthesized simultaneously, or 1-12 samples can be synthesized separately. 12. Automatic protection function: When a certain system fails in temperature control and pressure control, the instrument will automatically cut off the microwave transmission and alarm; 13. Self-locking buffer explosion-proof furnace door, when the reaction is abnormal, the buffer structure ensures the personal safety of the operator and the structure of the furnace door is intact; 14. The air chamber has a air-cooling function, which continuously cools the reaction tank, and the temperature and pressure are displayed in real time. 15. The furnace chamber is equipped with a high-power exhaust system, and various reactions can be continuously performed for a long time in a ventilated, safe and easy-to-view environment. The furnace chamber is ventilated with acid-resistant, high-volume centrifugal fan, and the exhaust air volume is not less than 5m3/min; 16. Control the operating system and the host computer are separate, and can be operated and controlled at a distance, which can ensure personal safety. 17. Microwave leakage complies with national standards;
Introduction: The instrument adopts microwave non-pulse continuous automatic frequency conversion control to extend the service life of the instrument and the uniformity of electromagnetic waves. The cavity is made of 52L large volume 316L stainless steel cavity material, and the self-locking buffer explosion-proof furnace door, when the reaction is abnormal, The buffer structure ensures the operator's personal safety and the structure of the furnace door is intact, the furnace door and the cavity are tightly combined, and the microwave leakage complies with national standards. The instrument uses a temperature and pressure dual control system to control the pressure and temperature of the synthesis experiment and display it in real time. The 360° round-trip continuous rotation and uniform microwave ensure the same microwave environment of each sample and improve the consistency of experimental results. When the pressure in the tank exceeds the set protection value, the microwave will automatically stop heating. The safety explosion-proof membrane has a double safety function. When the pressure inside the tank exceeds the pressure that the explosion-proof membrane can withstand, the explosion-proof membrane first ruptures, and the gas vents to prevent damage to the tank and damage to the human body.
