Introduction: Microwave chemical synthesizer, suitable for chemical synthesis extraction reaction in microwave environment under normal pressure; suitable for chemical research (organic synthesis chemistry, inorganic chemistry, analytical chemistry, medicinal chemistry, military chemistry), biomedicine, material science , food science, inspection and quarantine, petrochemical industry, and agriculture, forestry and fishery testing fields; the physical and chemical processes in the synthesis and extraction process are accelerated by microwave energy. In many application fields, microwave energy can greatly improve the reaction speed and reduce the reaction temperature. At the same time, it is easy to complete the synthesis process that the traditional synthesis reaction method is relatively difficult to complete. Features: 1. Open atmospheric pressure microwave chemistry platform 2. Support 500ml three-necked flask reaction system within 300˚C 3. Support condensation reflux process 4. Support mechanical and electromagnetic double stirring 5. Intelligent control system, temperature and power closed-loop controllable 6. The experimental data curve is displayed and the data can be exported 7. User-customized and expandable functions: 1000W high power, 500˚C reaction system, 1000ml reactor Technical parameter: microwave system 1. Microwave power: rated power 800W/2450MHz, stepless non-pulse continuous microwave power output 2. Design of microwave reaction cavity: ①304 stainless steel is welded together, which is strong and reliable; ②The inner surface is coated with multi-layer Teflon anti-corrosion coating, which is suitable for use in acid-base corrosion and high-temperature environments, and is easy to wipe and clean 3. Inner cavity size: about 20L, of which the design with a height of 275mm is suitable for the process assembly of various vertical reaction vessels functional system 1. Reaction system: 500ml glass three-necked flask, open reaction system, supports temperature measurement, stirring, condensation and reflux functions 2. Temperature control: ①Temperature range: common working temperature is 0~300℃; ②Using thermocouple temperature measurement, plug-in temperature measurement method 3. Mixing control: double stirring mode of mechanical stirring and magnetic stirring 4. Mechanical stirring: Teflon anchor stirrer is used, driven by a speed regulating motor, and the speed is adjustable 5. Magnetic stirring: Teflon wrapped rotor, magnetic drive, adjustable speed 6. Process monitoring: ①The interior of the microwave cavity is equipped with LED spotlights, and the working conditions in the furnace cavity are monitored through the observation window of the door body ②Set up color video to monitor the reaction of internal materials, and you can understand the working status of the reaction system through the video Control System 1. Using PLC programming control: good human-computer interaction, integrated control terminal, intelligent and controllable temperature and power 2. Touch screen dialogue window, easy and fast operation, real-time display of time, temperature, power curve, data can be read and stored 3. Multiple sets of program memory functions, which can store, modify, call, delete and other system operations according to the program. security system 1. The door body has multiple interlocking structure, the door is powered off, and the operator is protected 2. The door body adopts a pull-down locking structure, which has the function of elastic translation and pressure relief to protect the operator. 3. The door body adopts λ/4 high impedance microwave anti-current suppression structure to ensure the health and safety of operators. Microwave leakage: <5mW/cm2 (better than the national standard) 4. The equipment is equipped with a negative pressure fan, which can quickly remove the exhaust gas in the furnace cavity and protect the operator Machine description 1. Equipment power supply: 220Vac / 50Hz, power consumption of the whole machine: 1300W 2. Equipment water supply: cold water system (condensation recovery process) 3. Appearance dimensions: (1) Approx. main body: 782×492×450mm (W×H×D), (2) Approx. top bracket: 500mm 4. Equipment weight: 50kg
Introduction: Microwave chemical synthesizer, suitable for chemical synthesis extraction reaction in microwave environment under normal pressure; suitable for chemical research (organic synthesis chemistry, inorganic chemistry, analytical chemistry, medicinal chemistry, military chemistry), biomedicine, material science , food science, inspection and quarantine, petrochemical industry, and agriculture, forestry and fishery testing fields; the physical and chemical processes in the synthesis and extraction process are accelerated by microwave energy. In many application fields, microwave energy can greatly improve the reaction speed and reduce the reaction temperature. At the same time, it is easy to complete the synthesis process that the traditional synthesis reaction method is relatively difficult to complete.